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Public Center for Instrumental Analysis of XJTU-SCET

Contact person: date: 2018-12-24

The center for instrumental analysis of XJTU-SCET was established in July, 2017. At present, it has opened and shared 22 instruments and equipment whose models and specifications are given as follows.

Instruments

Model & Specification

Photo

Field Emission Scanning Electron Microscope (FESEM)

TESCAN MAIA3LMH

resolution:0.7nm@15kV,1.0nm@1kV

acceleration voltage:0.2-30 kV

amplification: 4×~1,000,000

accessory:EDS and metal spraying

X-Ray Diffractometor (XRD)

Shimadzu XRD-6100

range:6°-148°,

min step:0.0001°

type:powder, film and any materials that are difficult to fix.

FourierTransformInfraredSpectrometer(FTIR)

Nicolet iS50

range:4000–400 cm-1

function:ATR, transmission, diffuse reflection and in situ infrared.

IonChromatograph

Thermo Scientific-Integrion

function:It can determine the anion content in pure water, including F-, Cl-, Br-, SO42-, NO3-, PO43-,Li+, Na+, K+, Ca2+, Mg2+, NH4+

level:ppm

Elemental Analysis

ELEMENT

function:Content analysis of non-metallic elements (including five elements C, H, N, S and O).

range:C:0.03-20mg;H:0.03-3mg;N:0.03-2mg;S:0.03-6mg;O:0.03-2mg

Full Range Chromatograph for Oil

JAS,based on Agilent 7890

function:It can determine the distillation process of raw oil or product oil.

Specific Surface Area and Porosity Analyzer

McKiebel BELSORP-Max

function: It can realize simultaneous measurement of microhole, three-station specific surface and mesoporous, and can test specific surface area (SSA) and aperture analysis (including pore volume, pore size distribution, average pore size, etc.).

Chemical Adsorption Instrument

Quantachrome-Autosorb-iQC-TPX

function:dynamic chemical adsorption: TPD, TPR, TPO, pulse titration.

Simultaneous TG-DSC Apparatus

NETZSCH-STA449F5

function:simultaneously get the TGA and DSC signals of the samples at the room temperature to 1600℃.

Optical Contact Angle Measuring Device

KRÜSS-DSA100

function:it can measure the contact Angle between liquid solid, analyze solid surface free energy, measure the static contact Angle, Angle and back Angle, which can realize the constant temperature measurement from room temperature to 130℃.

Atomic Absorption Spectrophotometer

(AAS)

Shimadzu AA-6880

function:it can measure the content of Fe、Mn、Na、Mg、K、Ca、Cu、Ag in aqueous solution.

accuracy:ppm for flame method and ppb for graphite furnace method.

Nano particle size and zeta potential analyzer

Malvern Zetasizer Nano ZSE

function:it can measure the particle size (0.3 nanometer to 10 micron), Zeta potential (mpt-2 multi-purpose three-part automatic titrator) and absolute molecular weight.

Laser Particle Size Analyzer

(LPSA)

OMEC LS-909

Range:0.02~2100μm(wet process)、0.1~2100μm(dry process)

Electrochemical Workstation

Princeton- VersaStudio

function:Volt-ampere technology, corrosion technology, energy technology and alternating current impedance technology

Scanning Electrochemical Microscopy

(SECM)

Princeton

VersaSCAN-VersaStat3 /3F

Function: It can study the local electrochemical reactions, obtain the electrochemical parameters of each measured position and create a data schematic of local current by scanning the measurement probe. It can also study the volt-ampere technology, corrosion technology, energy technology and alternating current impedance technology

Steady-state Surface Photovoltage Spectrometer

CHF-XM-500W

Function: Photovoltage measurement, photocurrent measurement, photovoltaic phase spectrum, photoelectric conversion efficiency (IPCE)

On-line Gas Mass Spectrometers

Pfeiffer-GSD32002OmniStar;

TILON-LC-D200M

Range: 1-200amu,

Function: residual gas analysis (RGA), catalytic research (TPR, TPD, TPO), environmental exhaust analysis, gas purity analysis, reaction kinetics, etc.

Vacuum Sputtering Plating Machine

MSP-300B

function:coating by direct current sputtering, radio frequency sputtering, oblique target co-sputtering and vertical sputtering. The target materials include Al, Cu, Ti and graphite.

Slow Strain Rate Tensile Stress Corrosion Tester

CRIMS MFDL100-100KN

Max load:100KN;

drawing rate:0.00000001/s~0.000001/s;

Max travel of pull rod:180mm

Electo-hydraulic Servocontrolled Fatigue Testing Machine

CRIMS SDS100-100KN

Maximum static test force

:±100kN;

Maximum dynamic test force:±80KN;Actuator effective travel

:±50mm

Highspeed Camera

Japan-NAC

Light source:Montedison Video light LED-V200;

Lens:Nikon 24-85mm f/2.8-4D and Nikon 80-200mm f/2.8D;

Spider:Manfrotto 475B;

Holder:Manfrotto 808RC4

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